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alt="產(chǎn)品5.jpg" title="產(chǎn)品5.jpg" la="la"/> </div> </li> </ul> </div> </div>  <div id="nxjnchi" class="magnifier-view"></div> </div> </div></div> <div id="sxj3c2g" class="cbox-2-1 p_item"><div id="vfr7apo" class="e_container-3 s_layout"> <div id="8bvejnh" class="cbox-3-0 p_item"><p class="e_text-4 s_title"> 4J29 </p><p class="e_text-5 s_title"> 一、概述?1.14J29材料牌號4J29。1.24J29相近牌號見(jiàn)表1-1。?1.34J29材料的技術(shù)標準YB/T5231-1993《鐵鎳鈷玻封合金4J29和4J44技術(shù)條件》。1.44J29化學(xué)成分見(jiàn)表1-2。在平均線(xiàn)膨脹系數達到標準規定條件下，允許鎳、鈷含量偏離表1-2規定范圍。鋁、鎂、鋯和鈦的含量各不大于0.10%，其總量應不大于0.20%。1.54J29熱處理制度標準規定的膨脹系數及低溫組 </p><div id="kelke2t" class="e_loop_sub-27 s_list wy_flexWrap wy_flexAcenter"> <span style="font-size:var(--wy_FSSix);color:#333;">所屬分類(lèi)：</span> <div id="mkgazvm" class="cbox-27 p_loopItem"><p class="e_text-28 s_title"> <a href="/product/精密合金-8" target="_self"> 精密合金 </a> </p></div> <div id="u3eosed" class="cbox-27 p_loopItem"><p class="e_text-28 s_title"> <a href="/products/2.html" target="_self"> 首頁(yè)產(chǎn)品 </a> </p></div> </div><hr class="e_line-12 s_line" /><a class="e_button-6 s_button2 btn btn-primary " href="/contact.html" target="_self"> <span>聯(lián)系我們</span> </a> <a class="e_button-29 s_button2 btn btn-primary " href="#cp_Message" target="_self"> <span>在線(xiàn)留言</span> </a> </div> </div></div> </div><div id="vhvu3gf" class="e_container-13 s_layout"> <div id="8fkt8cg" class="cbox-13-0 p_item"><div id="d887c22" class="e_container-17 s_layout"> <div id="ptsrvf3" class="cbox-17-0 p_item"><div id="pe2p37w" class="e_container-16 s_layout"> <div id="mvodc8g" class="cbox-16-0 p_item"><p class="e_text-15 s_title"> 產(chǎn)品描述 </p></div> </div></div> </div><div id="v38yxmv" class="e_richText-14 s_title"> <div id="esmo3y7" class="reset_style js-reset_style js-adapMobile "> <div><img alt="" class="imageResponse js-onerror" domain-src="/repository/image/EiYn6sRfQxO-pTSlbpPvJg.jpg" id="1413" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/744fff8e-af4f-4fda-b01e-650ef6807926.jpg" style="width: 776px; height: 557px;" /></div> <div> </div> <div><span style="color:#6cc9f2;"><span style="font-size:18px;"><strong>一、概述</strong></span></span></div> <div> </div> <div>1.1 4J29材料牌號 4J29。</div> <div>1.2 4J29相近牌號見(jiàn)表1-1。</div> <div> </div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/rtdSwtFRSD2YLfA3JyLRcg.jpg" id="87" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/505616ee-dbbb-4360-8ef8-f668bb8efb34.jpg" /></div> <div>1.3 4J29材料的技術(shù)標準 YB/T 5231-1993《鐵鎳鈷玻封合金4J29和4J44技術(shù)條件》。</div> <div>1.4 4J29化學(xué)成分見(jiàn)表1-2。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/F7M1wUZ5SXKAthwM1ThHNw.jpg" id="90" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/8edef5aa-7a4c-4f87-914e-c57d16708569.jpg" /></div> <div>在平均線(xiàn)膨脹系數達到標準規定條件下，允許鎳、鈷含量偏離表1-2規定范圍。鋁、鎂、鋯和鈦的含量各不大于0.10%，其總量應不大于0.20%。</div> <div>1.5 4J29熱處理制度標準規定的膨脹系數及低溫組織穩定性的性能檢驗試樣，在氫氣氣氛中加熱至900℃±20℃,保溫1h，再加熱至1100℃±20℃，保溫15min，以不大于5℃/min速度冷至200℃以下出爐。</div> <div>1.6 4J29品種規格與供應狀態(tài) 品種有絲、帶、板、管和棒材。</div> <div>1.7 4J29熔煉與鑄造工藝用非真空感應爐、真空感應爐或電弧爐熔煉。</div> <div>1.8 4J29應用概況與特殊要求該合金是國際通用的典型的Fe-Ni-Co硬玻璃封接合金。經(jīng)航空工廠(chǎng)長(cháng)期使用，性能穩定。主要用于電真空元器件如發(fā)射管、振蕩管、引燃管、磁控管、晶體管、密封插頭、繼電器、集成電路的引出線(xiàn)、底盤(pán)、外殼、支架等的玻璃封接。在應用中應使選用的玻璃與合金的膨脹系數相匹配。根據使用溫度嚴格檢驗其低溫組織穩定性。在加工過(guò)程中應進(jìn)行適當的熱處理，以保證材料具有良好的深沖引伸性能。當使用鍛材時(shí)應嚴格檢驗其氣密性。</div> <div> </div> <div><span style="color:#6cc9f2;"><span style="font-size:18px;"><strong>二、4J29物理及化學(xué)性能</strong></span></span></div> <div>2.1 4J29熱性能 </div> <div>2.1.1 4J29溶化溫度范圍該合金溶化溫度約為1450℃[1,2]。</div> <div>2.1.2 4J29熱導率見(jiàn)表2-1。</div> <div> </div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/zFguO0PlRfyA0t2a6dXbJw.jpg" id="92" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/c075a570-940a-4a12-9c9b-6be8375cf2ea.jpg" /></div> <div>2.1.3 4J29比熱容在0℃時(shí)，比熱容為440J/(kg•℃)；在430℃時(shí)，比熱容為649J/(kg•℃)。</div> <div>2.1.4 4J29線(xiàn)膨脹系數標準規定α1(20～400℃)=(4.6～5.2)×10-6℃-1；α1(20～450℃)=(5.1～5.5)×10-6℃-1(當用于晶體管時(shí)上限為5.6×10-6℃-1)。</div> <div>合金的平均線(xiàn)膨脹系數見(jiàn)表2-2。合金的膨脹曲線(xiàn)見(jiàn)圖2-1。</div> <div> </div> <div><strong><img class="imageResponse js-onerror" domain-src="/repository/image/zBwDgVMnRmmLs4TzAskqEw.jpg" id="93" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/2c27f791-7886-471d-a2ba-8a177a7490da.jpg" /></strong></div> <div>2.2 4J29密度</div> <div>2.3 4J29電性能</div> <div>2.3.1 4J29電阻率 ρ=0.48μΩ·m[1,5]。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/BTQlSXGSTWik69Jk8X3jBg.jpg" id="94" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/423e92ed-50c2-4609-a1b1-fd744ae5828f.jpg" /></div> <div><span style="font-size: 12pt;">2.3.1 4J29電阻溫度系數見(jiàn)表2-3。</span></div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/bILGR-37QACDFzXt9hqT4A.jpg" id="97" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/b5cf6a90-1827-4a42-9fc5-4cc5fd68439d.jpg" /></div> <div>2.4 4J29磁性能</div> <div>2.4.1 4J29居里點(diǎn) Tc=430℃[1,5]。</div> <div>2.4.2 4J29合金的磁性能見(jiàn)表2-4[1]。</div> <div>在4000A/m下，剩余磁感應強度Br=0.98T，矯頑力Hc=68.8A/m[1,2]。</div> <div>2.5 4J29化學(xué)性能合金在大氣、淡水和海水中有較好的耐腐蝕性。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/M7K5ZTGnTkqjVajDUfOP6Q.jpg" id="98" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/b01aefe4-03c2-46f6-b055-36fd9145be0b.jpg" /></div> <div> </div> <div><span style="color:#6cc9f2;"><span style="font-size:18px;"><strong>三、4J29力學(xué)性能</strong></span></span></div> <div> </div> <div>3.1 4J29技術(shù)標準規定的性能</div> <div>3.1.1 4J29硬度深沖態(tài)帶材的硬度應符合表3-1的規定。厚度不大于0.2mm時(shí)不作硬度檢驗。</div> <div>3.1.2 4J29抗拉強度絲材和帶材的抗拉強度應符合表3-2的規定。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/1oNI-oBqQZ6Jg0jKa-uOtw.jpg" id="99" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/690bbc75-3dbe-414e-a10c-6fbb31772c51.jpg" /></div> <div>3.2 4J29室溫及各種溫度下的力學(xué)性能</div> <div>3.2.1 4J29硬度冷應變率為50%的帶材，在不同退火溫度下的硬度見(jiàn)圖3-1。</div> <div>3.2.2 4J29拉伸性能合金（退火態(tài)）在室溫的拉伸性能見(jiàn)表3-3。冷應變率為50%的帶材，在不同退火溫度下的拉伸性能見(jiàn)圖3-2。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/ANKm9qB7RmGtTwtxg364TA.jpg" id="101" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/35320a3b-f925-40e9-9f28-9c57db880a9a.jpg" /></div> <div> </div> <div>3.3 4J29持久和蠕變性能</div> <div>3.4 4J29疲勞性能 </div> <div>3.5 4J29彈性性能 </div> <div>3.5.1 4J29彈性模量 E=138GPa。</div> <div> </div> <div><span style="color:#6cc9f2;"><span style="font-size:18px;"><strong>四、4J29組織結構</strong></span></span></div> <div> </div> <div>4.1 4J29相變溫度 γ→α相變溫度在-80℃以下。 </div> <div>4.2 4J29時(shí)間-溫度-組織轉變曲線(xiàn) </div> <div>4.3 4J29合金組織結構合金按1.5規定的熱處理制度處理后，再經(jīng)-78.5℃冷凍，大于等于4h不應出現馬氏體組織。但當合金成分不當時(shí)，在常溫或低溫下將發(fā)生不同程度的奧氏體(γ)向針狀馬氏體(α)轉變，相變時(shí)伴隨著(zhù)體積膨脹效應。合金的膨脹系數相應增高，致使封接件的內應力劇增，甚至造成部分損壞。影響合金低溫組織穩定性的主要因素是合金的化學(xué)成分。從Fe-Ni-Co三元相圖中可以看到，鎳是穩定γ相的主要元素，鎳含量偏高有利于γ相的穩定。隨合金總變形率增加其組織越趨向穩定。合金成分偏析也可能造成局部區域的γ→α相變。此外晶粒粗大也會(huì )促進(jìn)γ→α相變。</div> <div>4.4 4J29晶粒度標準規定深沖態(tài)帶材的晶粒度應不小于7級，小于7級的晶粒不得超過(guò)面積的10%。厚度小于0.13mm的帶材估計平均晶粒度時(shí)，沿帶材厚度方向晶粒個(gè)數應不少于8個(gè)。</div> <div>冷應變率為60%～70%的厚的帶材，在表4-1所示溫度下退火1h,空冷后，按YB 027-1992附錄A評級，其晶粒度見(jiàn)表4-1。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/33CPubT3S0ambXDFRGxA1Q.jpg" id="102" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/8d91d18f-2f7e-41f3-87fd-12dbc66a6675.jpg" /></div> <div> </div> <div><span style="color:#6cc9f2;"><span style="font-size:18px;"><strong>五、4J29工藝性能與要求</strong></span></span></div> <div>5.1 4J29成形性能該合金具有良好的冷、熱加工性能，可制成各種復雜形狀的零件。但應避免在含硫的氣氛中加熱。在冷軋時(shí)，當帶材的冷應變率大于70%時(shí)，退火后會(huì )引起塑性各向異性；冷應變率在10%～15%范圍時(shí)，合金在退火后會(huì )導致晶粒急劇長(cháng)大，也將產(chǎn)生合金的塑性各向異性。當最終應變率為60%～65%，晶粒度為7～8.5級時(shí)，其塑性各向異性最小[2,4,7～9]。</div> <div>合金帶材的杯突值與厚度的關(guān)系見(jiàn)圖5-1。</div> <div><img class="imageResponse js-onerror" domain-src="/repository/image/2VIPt1zHTMO-XgJ_5A9UNg.jpg" id="103" src="https://omo-oss-image.thefastimg.com/portal-saas/new2022080310181462570/cms/image/801710ec-3a3a-482d-9343-f9f210b6b4aa.jpg" /></div> <div> </div> <div>5.2 4J29焊接性能該合金可采用釬焊、熔焊、電阻焊等方法與銅、鋼、鎳等金屬焊接。當合金中鋯含量大于0.06%時(shí)，將影響板材的氬弧焊焊接質(zhì)量，甚至使焊縫開(kāi)裂。</div> <div>該合金與玻璃封接前，應清洗干凈，隨后進(jìn)行高溫濕氫處理、預氧化處理。</div> <div>5.3 4J29零件熱處理工藝熱處理可分為：消除應力退火、中間退火、凈化去氣處理、預氧化處理。</div> <div>(1)消除應力退火為消除零件在機械加工后的殘存應力要進(jìn)行消除應力退火：470～540℃，保溫1～2h,爐冷或空冷。</div> <div>(2)中間退火為消除合金在冷軋、冷拔、冷沖壓過(guò)程中引起的加工硬化現象，以利于繼續加工。工件需在干氫、分解氨或真空中，加熱到750～900℃，保溫14min～1h，然后爐冷，空冷或水淬。</div> <div>(3)凈化去氣處理零件成形后，預氧化處理前，需進(jìn)行濕氫處理，處理前應進(jìn)行除油。工作需在飽和濕氫中，加熱到950～1050℃，保溫10～30min,然后爐冷。</div> <div> </div> <div>(4)預氧化處理合金在濕氫處理后，熔封前一般要進(jìn)行預氧化處理，使合金表面生成一層厚度均勻、致密的氧化膜，該氧化膜與基體結合牢固，且能很好地與熔融的玻璃浸潤。零件在濕氫處理后，在大約800℃的空氣中氧化。零件的增重在0.2～0.4mg/cm2范圍為宜[10]。</div> <div>該合金不能用熱處理硬化。</div> <div>5.4 4J29表面處理工藝表面處理可用噴砂、拋光、酸洗。</div> <div>零件與玻璃封接后，為易于焊接，需去除封接時(shí)生成的氧化膜，可將零件在10%鹽酸+10%硝酸的水溶液中，加熱到70℃左右，酸洗2～5min。</div> <div>該合金具有良好的電鍍性能，表面能鍍金、銀、鎳、鉻等金屬。為便于零件間的焊接或熱壓粘結，常鍍以銅、鎳、金、錫的鍍層。為改善高頻電流的傳導能力，降低接觸電阻以保證正常的陰極發(fā)射特性，常鍍以金、銀的鍍層。為提高器件的耐蝕性能可鍍鎳或金[11]。</div> <div>5.5 4J29切削加工與磨削性能該合金切削特性和奧氏體不銹鋼相似。加工時(shí)采用高速鋼或硬質(zhì)合金刀具，低速切削加工。切削時(shí)可使用冷卻劑。該合金磨削性能良好。</div> </div> </div><div id="hh2let8" class="e_container-45 s_layout"> <div id="ya38jic" class="cbox-45-0 p_item"><div 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